Preliminary tests of synthetic organic compounds as insecticides

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Title:
Preliminary tests of synthetic organic compounds as insecticides
Physical Description:
134 p. : ; 27 cm.
Language:
English
Creator:
Swingle, M. C
Phillips, Arthur M., 1903-
Gahan, J. B
United States -- Bureau of Entomology and Plant Quarantine
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U.S. Department of Agriculture, Agricultural Research Administration, Bureau of Entomology and Plant Quarantine
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Washington, D.C
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Subjects / Keywords:
Insecticides -- Testing   ( lcsh )
Organic compounds -- Synthesis   ( lcsh )
Insecticides -- Testing   ( fast )
Organic compounds -- Synthesis   ( fast )
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federal government publication   ( marcgt )
bibliography   ( marcgt )
non-fiction   ( marcgt )

Notes

Bibliography:
Includes bibliographical references (p. 5-6).
Statement of Responsibility:
M.C. Swingle, A.M. Phillips, and J.B. Gahan.
General Note:
Caption title.
General Note:
"E-621."
General Note:
"July 1944."

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Source Institution:
University of Florida
Rights Management:
All applicable rights reserved by the source institution and holding location.
Resource Identifier:
oclc - 779542705
ocn779542705
System ID:
AA00025650:00001

Full Text
LIBRARY

STATE PLANT BOARD

July 19q44 E-621

UNITED STATES DARTENT OF AGRICULTURE Agricultural Research Administration Bureau of Entomology and Plant Quarantine

PRELIMINARY TESTS OF SYNTHETIC ORGANIC
COMPOUNDS AS INSECTICIDES. PAI~T I. 1/

M. C. Swingle A. M. Phillips 3.1, and J. B. Ghan Division of Control Investigations


In 1941 the authors published a description (j) of certain methods
and equipment used at the insecticide testing laboratory of the Bureau of Entomology and Plant Quarantine at Sanford,, Fla. A large number of
synthetic organic compounds have been evaluated as insecticides by these
test methods, and the present paper summarizes the results obtained on
883 compounds that were tested from July 1937 to October 1939.

The present paper deals only with preliminary tests, in which no
attempt was made to determine lethal doses or comparative toxicity.
They were made under conditions allowing fairly normal reaction by the
insects, and the data merely indicate those compounds that may have
potential insecticidal value. Materials showing toxicity in these tests
were set aside for later, more specialized tests to determine their
utility as spray deposits on potted plants, effect on tender foliage,
stability to outdoor exposure, and other information important to their
practical use.

Twenty species of insects were used in these tests. Not all of
the compounds were tested on every species, but in general more insects
were used with the more toxic materials.



if Most of the materials tested were furnished by the Division of
Insecticide Investigations, and many of them have been patented PA
insecticides by members of that Division. The writers wish to acknowledge the assistance of R. C.Roark, H. L. Hailer, C. M. Smith, and other members
of that Division who supplied the samples for testir, an1 especially of
C. V. ?owan, who furnished the formulas and other inforrntion on the
characteristics of the mat-rials.

2/ Resigned December 18, 1043.

3] Now with the Division of Fruit Insect Inrestigations.

i/ Now with the Division of Insects Affecting Man and Animals,






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The following insects were used:

American cockroach (Periplaneta americana (L.))
Australian cockroach (Periplaneta australasiae (F.))
Bean leaf roller (Urbanus proteus (L.))
Cabbage aphid (Brevicoryne brassicae (L.))
Cabbage looper (Autographa brassicae (Riley))
Cabbage webworm (Hellula undalis (F.))
Colorado potato beetle (Leptinotarsa decemlineata (Say))
Cowpea weevil (Callosobruchus maculatus (F.))
Cross-striped cabbage worm (Evergestis rimosalis (Guen.))
Diamondback moth (Plutella maculipennis (Curt.))
Fall webworm (Hyphantria cunes (Drury))
Greenhouse leaf tier (Phl ctaenia rubigal.is (Guen.))
Hawaiian beet webworm (Hymenia fascialis (Cram.))
Imported cabbage worm (Pieris rapae (L.))
Melon worm (Diphania hyalinsta L.))
Rice weevil (Sitophilus orza (L.))
Southern armyworm (Prodenia eridania (Cram.))
Southern beet webworm (Pehsancla bipunctalis (F.))
Termites (Reticulitermes sp.)
Yellow woolly bear (Diacrisia virginica (F.))

All the species except the bean leaf roller, the cabbage aphid, and termites were reared in the laboratory, in order to standardize the population and to insure their availability when desired.

The results obtained in an insecticide-testing program will depend upon the test insects. If a number of species are used, the general results are less variable and the compounds may be judged not only on the mortality caused but also on their effectiveness against species of varying resistance, An estimate based on the results obtained with 10 standard insecticides (table 1) shows the order of susceptibility of the 10 species most commonly used (larval stage) to be approximately as follows: Colorado potato beetle, diamondback moth, southern beet webworm, crossstriped cabbage worm, Hawaiian beet webworm, esolon worm, cabbage looper, fall webworm, southern armyworm, and greenhouse leaf tier.

Many of the samples received for testing were without physical
preparation to reduce them to a particle size similar to that of commercial insecticides. When necessary, materials were ground in a mortar to obtain a duetable sample, but in some cases this improved the
samples only slightly. In general the particle size was much larger than that of commercial insecticides, and this fact must be considered
when appraising these results.








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METHODS OF TESTING

Leaf.-.eeding Insects.-The first tests with leaf-feeding insects were made by feeding to larvae leaf sections that had been rather heavily dusted with *the undiluted material. For most of the tests three leaf sections about 2 inches square were used. The dust was applied in a settling chamber (1) to both surfaces of the leaves, and the amount was determined by weighing an aluminum plate dusted at the same time. Each leaf section wa~s then placed in a 9-cm. Petri dish
together with 10 nearly full grown larvae. After 145 hours the dishes were examined for dead larvae and an estimate of the ,amount of feeding on the leaves.

The possibility of fumigation in these tests was easily determined by isolating a quantity of the material between two sheets of filter paper which were fitted into the lid of Petri dishes. The larvae were placed in the dish with untreated foliage.

To distinguish between contact and stomach action necessitated
a more elaborate technique than seemed warranted in these preliminary tests. This information was generally obtained later when extensive tests were made on the more toxic materiWa.

Cockroaches.-Most of the tests on cockroaches were made by
placing 10 roaches in a 7-inch-diameter battery jar containing a known quantity of the compound evenly distributed over the bottom. The jar* were coated with vaseline around the rim to prevent escape of the roaches. No food or water was placed in the jars.

Termites.-The method described by Hockenyos (14) was used in tests with termites. Forty grams of sandy soil, ground in a mortar with a weighed portion of th. insecticide, was placed in a 150-il. beaker containing 12 al. of water and a little paper tissue. When the soil had taken up the water, 30 to 140 termites of the worker caste were placed in each beaker. The beakers were held in a cabinet at 80 F.

Grain Weevils.-Many of the compounds were tested on rice weevils and cowpea weevils in Petri dishes with treated grain. A weighed portion of the insecticide was thoroughly mixed with 15 grams of wheat or peas by shaking in a small flask, and then placed in a Petri dish with 25 adult weevils. The dishes were held in a cabinet at 80 F. and after 2 and 4~ days examined for dead insects.


DISCUSSION 0OF RESULTS

Approximately 2 percent of the compounds tested were found to be very effective (90 to 100 percent mortality or no more than a trace of feeding) against all the leaf-feeding insects on which they were tested,










Seven percent of the compounds were effective against at least 60 percent of the species but were not found effective on them all. An additional 6 percent were effective against one or more species but not as many as 50 percent of those on which they were tested. Most of these toxic materials, however, were discarded after further testing. Many potential stomach insecticides were found to be too volatile for practical use, and other compounds that killed by fumigation in Petri dishes were not sufficiently volatile for practical use as fumigants. Injury to plant foliage was another common cause for rejection.

Table 2 includes all the compounds showing appreciable toxicity. Fourteen compounds were effective on all the leaf-feeding species on which they were tested. Eight of these were found to kill by fumigation p-bromo iodobenzene, p-chloro iodobensene, 2,5-dichloroanil ine, alpha, beta-dibromoethylbensene, o-nitrobromobenzene, o-nitrochlorobensene, p-nitrochlorobenzene, and o-nitroiodobenzene. The remaining six compounds were phthalonitrile, 4,6-dinitro-o-cresol, 4,6-dibromo-o-cresol,
o-nitroaniline, p-nitrobenzyl bromide, and alpha, beta-dibromo-betanitroethylbenzene. All but phthalonitrile and 4,6-dinitro-o-cresol were too volatile to be used as stomach insecticides. Phthalonitrile is slowly volatile, but extensive tests by the authors (8) have shown it to be rather effective as a stomach insecticide for use on foliage, equaling lead arsenate or derris in laboratory tests against certain insects. Dinitro-o-cresol is very toxic to insects but is injurious to foliage. It was found toxic to the codling moth by McAlister and Van Leeuven (a), and has been reported toxic to other insects by several workers. Most of the better compounds have been tested against the screwworm by Bushland (1) and against mosquito larvae by Fink and coworkers (2).

Sixty-two compounds in table 2 killed more than half the species on which they were tested but were ineffective against some. At least 20 percent of these are fumigants. Of the others, the better compounds are 1,4-diphenylsemicarbazide, p-aminoazobenzene, p-aminoazobenzene hydrochloride, diazoaminobenzene, 1,4~-dinitrosopiperazine, p-phenylenediamine, acetone semicarbazone, thiocoumarin, zanthydrol, hexachlorophenol, 2,4-dinitrophenol, and pentabromophenol. Extensive tests on 1,4-diphenylsemicarbazide have been made by the authors (n), and the compound has been found to equal lead arsenate as a stomach insecticide against certain insects in laboratory tests. A complete report of the tests with p-aminoazobenzene hydrochloride (6) shows this compound to be very effective against certain insects.

Approximately 60 additional samples in table 2 were effective against from 20 to 60 percent of the leaf-feeding insects against which they were tested. These are very specific materials and have definitely less value as insecticides.

Table 3 lists the compounds that were not toxic or showed only
slight toxicity. This table includes approximately 85 percent of the







-5


compounds tested. It is recognized that the table may contain a few materials worthy of inclusion in the more toxic groups had a greater number of tests been made.


SU)O4ART

The insecticidal action of 883 synthetic organic compounds has
been estimated by preliminary tests in the laboratory. Each compound was tested against 1 or more of 20 species, most of them leaf-.feeding insects, in order to evaluate their utility in the general field of insect control. The 25 most toxic compounds tested were as follows:

Acetone semicarbazone 1.,4-Dinitrosopiperazine
p-JAminoazobenzene Hexachlorophenol
p.Aminoazobenzene hydrochloride o-Nitroaniline
p-Bromo iodobenz en. p-Nitrobenzyl bromide
p-Chloro iodobenz en. o-Nitrobromobenz en.
Diazoaminobenzene o-Xitrochlorobenzen.,
4,6-P ibromo-o.-cresol p-.Nitrochlorobenzene
alpha, beta-Pibromoethylben: ene o-Nitro iodobenzene
alpha, beta-Dibromo-beta-n itroethylben: ens p-.Phenylenedliamine
2, 5.DIichloroaniline Phthalonitr ile
1 ,4-Diphenyl semicarbazide Thiocoujuarin
4 ,6-.Dinitro-o-cresol Xanthydrol
2, 4.-Ditrophenol


LITERATURE CITED

(1) Bushlandf R, C,,
1940. The toxicity of some organic compounds to young screwworms.
Jour. Econ. Ent. 33: 669-676.

(2) Fink, D. E., Smith, L. N., Vivian, D. L., and Claborn, H. V.
1~939. Toxicity tests with synthetic organic compounds against
culicine mosquito larvae. U. S. Bur. Ent. azd Plant
Q uar. Z-4~25, 34 -pp. [processed.]

(3) Cahan,, J. B., Swinigle, M. C., and Phillips, A. M4.
1c,41. l,4-Diphenyleemicarbazide as an ins-cticide. U. S. Bu-r.
r~nt. anid P19.nt Quar. E-549, 11 pp-. [P roceseedj

(4) hoclcenyos, G. L.
lp39. Laboratory evaluation of soil poiscL~a used! In termite
control. Jour. Econ. Ent. 32: 11-14q.

(5) McAlister, L. C., Jr., and Van Leeuwen., E. R.
1930. 1.aboratox- testr of miscellaneous mcnias ginst the
codling, mth. Jour, Econ. IEnt. ?








-6


(6) Phillips, A. M., Swingle, M. C., Gahan, J. B., and McGovren, E. R.
194l. p-Aminoazobenzene hydrochloride as an insecticide. U. S.
Bur. Ent. and Plant Quar. E-550, 8 pp. EPrcessed.7

(7) Swingle, M. C., Phillips, A. M., and Gahan, J. B.
1941. Laboratory testing of natural and synthetic organic substances as insecticides. Jour. Econ. Ent. 34: 95-99,
illus.

(8) Gahan, J. B., and Phillips, A. M.
1941. Phthalonitrile as an insecticide. U. S. Bur. Ent. and
Plant Quar. E-548, 12 pp. [Processed.







7



Table 1.-Results of laboratory toxicity tests of certain common
insecticides used as standards for comparing the
results obtained on new insecticidal compounds

Feed- Kill in,
Compound and Insect Stagel/ Foliage e/ Deposit 4 K .
inz/ Depsi hr
Micrograms Percent
per S. cm.
Barium fluosilicate
Cabbage looper Fifth Collards 1 100 90
Cross-striped cabbage worm First do. 1 180 81
do. Fourth do. 1 260 97
Hawaiian beet webworm do. Beet 1 170 100
Imported cabbage worm Second Collards 0 45 100
do. Third do. 0 45 100
Southern armyworm First do. 0 45 100
do. Second do. 1 45 96
Southern beet webworm Fourth Beet 1 170 100

Cryolite, natural
American cockroach Full grown 190 0
Cabbage looper Fifth Collards 2 125 50
Colorado potato beetle Fourth Potato 1 140 94
Cress-striped cabbage worm First Collards 1 170 8
do. Fourth do. 2 170 70
Diamondback moth do. do. 0 170 100
Fell webworm Fifth Pecan 3 140 0
Greenhouse leaf tier do. Collards 1 200 100
Hawaiian beet webworm Fourth Beet 2 155 77
Melon worm Fifth Pumpkin 1 210 100
Southern armyworm First Collards 0 85 100
do. Third do. 1 85 84
do. Fifth do. 3 85 0
Southern beet webworm Fourth Beet 1 125 93

Cryolite, synthetic
American cockroach Full grown 250 0
Cabbage looper Fifth Collards 1 345 84
Colorado potato beetle Fourth Pottto 1 110 100
Cross-striped cabbage worm First Collarde 0 250 100
do. Fourth do. 1 260 7
Diamondback moth Second do. 1 250 90
do. Fourth d6o. 1 250 70
Fall webworm do. Pecan 1 235 (72) 7


NAmbers refer to Lastar.

0 a no visible feeding, 1 trace. 2 = moderate. 3 w normal feeding.
comparable with that oq untreated foliage.

Numbers in parentheses indicate number of hours if not 4.









Table I.--(Continued)


Compound and Insect Stagel! Foliage Fen Deposit Killi
i n Eld' 8 bra.!/
Microirame
ep AQS. Percent

Cryolite, synthetic (Cont.)
Greenhouse leaf tier Fifth Collards 1 95 93
Hawaiian beet webworm Fourth Beet 1 125 97
Melon worm Fifth Pumpkin 1 310 100
Southern armyworm First Collards 0 170 100
do. Sixth do. 1 170 97
Southern beet webworm Fourth Beet 1 155 97

Cube root, powdered, 4.4% rotencne
American cockroach Full rown 460 30
Cabbage looper Fifth Collards 0 125 50
Colorado potato beetle Fourth Potato 1 140 100
Cross-striped cabbage worm do. Collards 1 125 100
Diamondback moth do. do. 0 140 100
Fall webworm do. Pecan 0 210 0
Greenhouse leaf tier Fifth Collards 2 280 3
Hawaiian beet webworm Fourth Beet 0 240 73
Melon worm Fifth Pumpkin 1 140 3
Southern armyworm First Collards 2 170 48
do. Third do. 2 170 7
Southern beet webworm Fourth Beet 0 280 76

Derris root,pawred ~ 4 rotexnne
American cocKroach Full grown 340 20
Cabbage looper Fifth Collards 1 140 67
Cabbage webworm Third do. 0 170 56
Colorado potato beetle Fourth Potato 1 125 100
Cross-striped cabbage worm do. Collards 1 185 53
Greenhouse leaf tier Fifth do. 2 250 0
Hawaiian beet webworm Fourth Beet 0 270 71
Imported cabbage worm Second Collards 0 75 100
do. Fourth do. 0 50 1-00
Melon worm Fifth Squash 1 230 60
Rice weevil Adult (Treated wbeat) 4/1: P 4
Southern armyworm First Collards 1 110 26
do. Third do. 3 110 0
do. Fifth do. 2 300 2
Termites Adult (Treated soil 1:200 80
do. do. do. 11I000 0



All proportions by weight.






9

Table 1.--( Continued)

Compound and Insect Stpgel/ Foliage Deposit 4Kill

Pm.L_ 31-&. Percent

Lead arsenate
Bean leaf roller Fourth Bean 1 130 86
Cabbage looper Fifth Collards 2 95 50
Colorado potato beetle Fourth Potato 1 60 97
Cross-striped cabbage worm First Collards 0 70 100
do. Fourth do. 1 70 66
Diamondback moth Second do. 0 60 100
do. Fourth do. 0 60 87
Fall webworm Fifth Pecan 3 80 (72) 7
Greenhouse leaf tier do. Collards 1 140 100
Hawaiian beet webworm fourth Beet 1 125 51
Melon worm Fifth Pumpkin 1 130 97
Southern armyworm First Collards 0 70 100
do. Fourth do. 1 70 22
Southern beet webvorm do. Beet 1 110 53

Paris green
American cockroach Full grown 400 45
Cabbage looper Fifth Collards 0 260 100
Colorado potato beetle Fourth Potato 1 200 100
Cross-striped cabbage worm First Collards 0 250 100
do. Fourth do. 1 250 96
Diamondback moth Second do. 0 250 100
do. Fourth do. 0 250 97
Fall webworm Fifth Pecan 0 295 (72) 100
Greenhouse leaf tier 4d. Collards 0 325 100
Hawaiian beet webworm Fourth Beet 1 185 100
Melon worm Fifth Pumpkin 0 155 93
Southern armyworm Sixth Collards 1 230 100
Southern beet vebworm Fourth Beet 1 185 100

Phenothiazine, 6 4

American cockroach Pull gtown -- 3)0 20
Cabbage looper Fifth Collards 2 10 28
Colorado potato beetle Fourth Potato 1 110 33
Cros-striped cabbage worm Firqt Collards 0 95 100
do. Fourth do. 1 95 23
Diamondback moth Second do. 0 180 100
do. Fourth do. 1 180 30
Fall webworm do. Pecan 0 230 (72) 7
Greenhouse leaf tier Fifth Collards 3 160 0
Hpwaiipn beet webworm d, Swiss chard 1 200 58
Melon worm do. Pimpkin 2 200 13
Rice weevil Adult (Treated ht) 1: 200T 16






10

Table l.--(Continued)

Compound and Insect Stagel/ Foliage Fee Deposit 48 hr
.icrograma
2** g.Percent
Phenothiazine, E NE6H4 (Cont.)

Southern armyworm First Collards 0 125 98
do. Third do. 1 125 43
Southern beet webworm Fourth Beet 1 170 58
Termites Adult (Treated soil) 1:1000 96
do. do. do. 1 2000 56
Pyrethrum: 0.3 pyrethrin I
03 pyrethrin II
American cockroach Full grown 310 60
Cabbage looper Fifth Collards 1 140 97
Cross-striped cabbage worm Fourth do. 0 230 100
Greenhouse leaf tier First do. 0 230 100
do. Fifth do. 1 295 83
Hawaiian beet webworm Fourth Beet 0 230 100
Imported cabbage worm Fifth Collards 2 170 72
Melon worm do. Pumpkin 1 155 66
Rice weevil Adult (Treatedwheat) 1:200 12
Southern armyworm First Collards 1 240 73
do. Fourth do. 2 240 10.
do. Sixth do. 3 370 0
Southern beet webworm Fourth Beet 0 215 94
Termites Adult Treated soil) 1:200 100
do. do. do. 1:1000 20

Sulfur
American cockroach Full grown 310 30
Cabbage looper Fifth Collards 3 140 0
Colorado potato beetle Fourth Potato 3 220 0
Cross-striped cabbage worm do. Collards 3 155 0
Diamondback moth do. do. 3 280 0
Fall webworin Fifth Pecan 3 185 0
Greenhouse leaf tier do. Collards 3 295 0
Hawaiian beet webworm Fourth Beet 3 260 0
Melon worm Fifth Pumpkin 3 230 0
Southern armyworm First Collarde 1 240 44
do. Third do. 1 240 3
Southern beet webworm Fourth Beet 3 230 0




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72


Table 3.-Experimental materials that were found to be nontoxic to the insects against which they were tested


Compound Insect Stage2

Acetaldehyde ammonia Cross-striped cabbage worm Fourth
CHC(0H)NH2 Southern armyworm Fifth


Acetamide Colorado potato beetle Fourth
CH 3CONE2 Greenhouse leaf tier Fifth
Melon worm Fourth
Southern armyworm do.
Southern beet webworm do.

m-Acrtamidobenzoic acid Greenhouse leaf tier Fourth
CH 3CONHC0HCOOH Hawaiian beet webworm Fifth
Melon worm Fourth
Southern armyworm Third
Southern beet webworm Fourth

2-Acetamidofluorene American cockroach 3/4 grown
SCGH4CH2CH3NHCOC3 Cabbage looper Fourth
Colorado potato beetle do.
Cross-striped cabbage worm do.
Greenhouse leaf tier Fifth
Hawaiian beet webworm do.
Melon worm Fourth
Rice weevil Adult
Southern armyworm First
do. Fifth
Southern beet webworm Fourth
Termites Adult
do. do.
do. do.

p-Acetaminobenzenesulfonanilide Colorado potato beetle Fourth
CH 3CONHC6H4SO2NRHC6H5 Cross-striped cabbage worm First
Melon worm Fifth
Southern armyworm First
do. Sixth

p-Acetamino-N-m-nitrophenylbenzene- Colorado potato beetle Fourth
sulfonamide Cross-striped cabbage worm do.
CH 3CONC H SO2 NHC H4 NO2



Numbers refer to instar.






T3
Table 3.- (Continued)


Compound Insect S tagel/


p-Acetamino -N-o-nitrophenylbenzene- Colorado potato beetle Fourth
sulffonamide Cr08-striped cabbage worm dio.
C3CONC6H4SO2NHC6H4NO2 Southern armyworm, do.

N(petaminohny1sulfonl)-morpholine Colorado potato beetle Fourth
OH3 COlNHC6HjfS2N(CH2CH2)20 Cross-striped cabbage worm do.
Melon worm Fifth
Southern armyworm Third

1-kcetanilidoben~oxazole do. sixth
11(c Co3) C6H5

m-Acetaniside Greenhouse leaf tier Fourth
oH3CNH64CH5 Hawaiian beet webworm Fifth
hielon worm Pourti
Southern armyworm Third
Southern beet webworm Fourth

o-Acetani side Hawaiian beet webworm Fifth
CH3CONRHC 40~CH3 Melon worm Fourth
Southern beet webworm do.

p-Acetaniside Greenhouse leaf tier Fourth
CH 3CO1NHC6H4OC1H3 Hawaiian beet webworu Fifth
Melon worm Fouirth
Southern armyworm Third
Southern beet webworm Fourth

A-cetoacetanilide Cross-striped cabbage worm Fourth
CH 3CO2CNGR Southern -rmywom, Sixth

Acetoacet-2,5-.dichloroanilide Cdabbage lootper First
Cl2C6 HCOC2CGcOCH 3 Crs-tripJ. cabb- worm Jo





Soathk rn arrnwor



3o Tird.
10.u r th
m-.Acetoto '1 Zy Ii de Iooad~ 1ot betl butL









Table 3.-.(Continued)


Compound Insect 6g~


N-.etylanthranilic acid Greenhouse leaf tier Fourth
CH O1H0CO Hawaiian beet webworm FiftVa
3 H~J)C0 Melon worm Fut
Southern armyworm Third
Southern beet webworm Fourth

Ace tylbenzoin Cabbage webworm Fourth
C 6H 5 COCH(C00CR3 )c C6H5 Cross-striped cabbage worm do.
Diamonidback moth do.
Greenhouse leaf tier Fif th
Hawaiian beet webworm do.
Melon worm do.
Southern armyworm Fourth
Southern beet webworm Fifth

9-Acetyl carbazol e Southern armyworm, First
Cg NOOCH 3do. Third
do. Fifth

Acetyldibenzofuran Diamondback moth Fourth
Cfl3C0CH0(6H4 Greenhouse leaf tier Fifth

lQ-Acetyl-5,5-dimethylacridan Cross-striped cabbage worm First
C614(00R) C6H4C( CR) Southern armyworm do.

Acetyl-41,6-dini tro-o-cresol do. Fifth
(NO 2)2 2C 6H2(OCOC C3) CR 3

Acetyldiphenylanine do. Second
(C6H5) 2NCOCH3

2-Acetyldiphenylene oxide Hawaiian beet webworm Fifth
Sm 06 H 3 0CR.H Melon worm Fourth
Southern armyworm First
do. Sixth
Southern beet webworm Fifth

N-Acetyl-alph..naphthyla.xine Colorado potato beetle .. Fourth
Cli CONRC H Cross-striped cabbage worm First
3 07Imported cabbage worm do.
Southern armyworm do.
do. Third

N-Acltyl-bet&..naphthylamine Cross-striped cabbage worm Fourth
CR 6ONHC10R 7 Southern armyworm Fifth







15

Table 3.- (Continued)


Compound Insect st age!/


Acetyl-p-phenetidifle Southern armyworm Fifth
CH 3COINEC0H4PC2H5 do. Sixth

6-.Acetylpheno thi azine do. Third
S00HC63 COCH3

I-Lcetylsulfanilamide Cross-striped cabbage worm First
CE 3CONH0S2H Southern armyworm do.

N-hcetyl sulfanil- ilph&r-uaphthylamlide Crosas-striped cabbage worm First
W3OH0SOMl" Southern armyworm do.
1-Acetyl sulfanil-p-nitroaiiilide Cross-striped cabbage worm First
Cz CO'M0WC40 do. Fourth
Imported cabbage worm First
Melon worm Fif th
Southern armyworii First

7-Acetyl-l, 2,3, 4-tetraydrodipheiylene do. sixth
oxide
CHG00CH OCIR
3 3 I6

Acetylurea Southern armyworm First
UH 2CONHCOCH 3

I-Acetyl-214--xylidine Cross-striped cabbage worm Fitrst
CHACOXHC 6H( CE -) P Southern Armiworm do.

C!1ldX Cross-striped cabbage worn, Fourth
C 6H,4C2C6RNM Melon wormFit
Southern axr1yworm Sixth

Acridone- Cross-striped cabbage worm First
LCi4,CO0041H Imported cabbage worm -do.
Southern armyworm o

Aii arin Cabba#'e we bworm Fourth
C6R2(OH)2(CO)2C694 Co-trpdCabb e worm do
Di on a k oth r
Gre~&~i~e1eI7tier Fo -r th
1,eloii worm Fif4-th
Southern irto Ywnrm Tid

Alai leSouthern beet w~bworm Fourth
(CHal blue CC Southern ariyworm First
(6H5 ~6a 4 2( ) C0HjnC6H4jSO9INa

Allanto in do. Stix:th
NECNO crri 0o







76

Table 3.- (Continued)



Compound Insect Stagel'


Allyl thiourea Cross-striped cabbage worm First
OH2: CHCH2NHfCSlH2 do. Fourth
Imported cabbage worm First
Southern armyworm do.
do. Fifth
do. Sixth

2-Aminoacridone Cross-striped cabbage worm First
4-Aminoac ri done Southern armyworm do.
C~~;U;"3N2)HImported cabbage worm d..

be ta-Ani no anthraquinone Colorado potato beetle Fourth
NH 206H3( O00)264 Cross-striped cabbage worm First
Imported cabbage worm do.
Southern armyworm, do.
do. Sixth

2-Amino-5-azoani sole Diaondback moth Fourth
C1I3OC63(NH2)N :NC0HG5ehos leaf tier Fifth
Hawaiian beet webworm, do.
Southern armyworm First
Southe rn beet webworm, Fifth

Aminoazobenzenesulfonic acid Southern armyworm First
COH5 :NC6H4NH2S03

2-Amino-5-azotoluene hydrochloride Croso-striped cabbage worm Fourth
CH 3C6HWNiCO3 (CH 3) NH2*HCIL Melon worm Fifth
Southern armyworm Third


p-Arinrobenzenesulfonanilide Colorado potato beetle Fourth
NH 2iC04SO 2NHC605 Cross-striped cabbage worm First
Southern armyworm do.

p-A~mintobenzenesu~ifonylitiide Colorado potato beetle Fourth
N-R2IO0NH2Cross-strir~ed cabbage worm First
Southern armyworm, do.
do. Sixth
m-Aminobenzoic acid Colorado potato beetle Fourth
p-Aminoberizoic acid Croso-striped cabbage worm do.
Ne 4;QUSouthern armyworm do.
P-A-minobenzophenone Cross-striped cabbage worm Fourth
0 H5 C0( 6 R R2 Melon worm Fif th
Southern armyworm Third






77
Table 3-- (Continued)


Compound Insect Stame-ij


4-AminodiphenvI,--iine s,ilfate Cross-striped cabbage worm Fourth
C6H5NK'-,0LXH2:R2S04 Melon worm Fif th
Southern armyworm Fou rth

6-Ar-ino-2.3-diphenylquinoxaline Cross-striped cabbage worm First
NH Southern arnyworm do

2-Amino-g-fluorenol Cabbage looper Fifth
C R CHOEC 6 H 3 NR 2 Southern arqMrm First
j6 4 CID Fourth
2-Aminofluorenone do. First
C6K4C0CaJ1NHr do. Fif th

2-Aminophenazine do. First
C6R4NC 6 R 3 ER 2 do. Third
do. Fifth

m-ilvdno-ohenol do. First
o-Aminoplenoi
HOC6#4M2

P-A,,inophenol Imported cabbage worm Fifth
HOC 6#002 -Sonthern armyworm Firnt
do. Fifth

5-Amino-l-phen.vlbenzothi; -zole Southern armywors First
,J1 C H -N: C(C R, ) S do. Fif th

7-Lz-ino-1,2,3,4-tetrehydrc'i.heni-lene do. sixth
oxide
NH C H Ocog
216 3
Aniline salt of 2.4-dinitro--;4-r hPkvla-ine-Crose-strined cabbage worm Fourth
6-carboxylic acid Southern arayworn Fifth
C 05 NRC 6 H 20KO 2)2 COOH KH 2CO 5

1 --ari 1i rib cen zo tz,-iazole do. Second
S H0:CNHC-,H, IC6 I v :I
1-Anilinobenzoxazole do. First
NHC6 H 5

3-Anilinophenothia7ine Cross-striped cabbage worm First
C ,H NH H 14;HC04S Inported cabbage worm io.
1) 5 2 6 3 Southern --rmrmrm cfo.






78

Table 3-- (continued)


Compound Insect Sta4ev

Anisal cinnamal acetone Cross-striped cabbage worm Fourth
CH OC6H4CHiCHCOCH:CHCE:CHC05 Melon worm Fifth
Southern armyworm Third

1-t(o-Anisylazo)-2-naphthol Southern armyworm First
C 30C6ENC10H60H do. Sixth

Anthracene do. Third
C6J4(C)2c6B

Anthragallol Cabbage webworw Fourth
0C14H502(o)3 Cross-striped cabbage worm do.
Diamondback moth Third
Greenhouse leaf tier Fourth
Melon worm do.
do. Fifth
Southern armyworm Third
do. Fourth
Southern beet webworm do.
Anthrahydroquinone diacetate Cross-striped cabbage worm Fourth
C6H4(COCOCH3)2C6H4 Melon worm Fifth
Southern armyworm Fourth

Anthraquinone Cabbage webworm Fourth
(C6H04)2(CO)2 Cross-striped cabbage worm do.
Diamondback moth Thiri
Greenhouse leaf tier Fourth
Melon worm do.
do. Fifth
Southern armyworm Fourth
Southern beet webworm do.
Anthraguinione-beta-sulfonic acid Cabbage webworm Fourth
CH CO)20 SO Cross-striped cabbage worm do.
Diamondback moth do.
Greenhouse leaf tier Fifth
Melon worm do.
Southern armyworm Fourth
Southern beet webworm Fifth
Anthranilic acid Southern armyworm Fourth
NE CHICO
NH2C6 OOH

Anthrone do. First
D do. Sixth
P04000 08do Sixth







79
Table 3-(Continued)


Compound Insect


Atovyl (sodium arsanilate) Southern armyworm Fifth
NK C6H4AsO3HNa,

4,4-Azobis(o-anisidine) Cross-stripedi cabbaee worm Fourth
M 0C K (NH )N :Nc H (NEH2)O Southern armnyworm Si -c-th

p,p'-Azobio(bexzoic acid) Colorado potato beetle Fourth
HOOCC6E4W :NC6H4COOR Cross-striped cabbpge worm do.
Melon worm Fifth
Southern armyworm do.

r~pt-.Azobi sbiphenyl Colorado potato beetle Fourth
OC H0N:"IC04jC65 Cross-striped cabbage worm do.
Melon worm Fifth
Southem armyworm do.

p~p'-Azobisphenetole Colorado potato beetle Fourth
C 25OC6H4N:NC6H4OC2H5 Cross-striped cabbage worm do.
Melon worm do.
Southern ar-,yworm Fifth

pop'-Azobispheno. Colorado potato beetle Fourth
HOC6HhN:WC HCH Cross-striped cabbage worm do.
Melon worm Fifth
Scuth-rn armyworm do.

A7.ochormi de do. do.


o-Lzothioani sole Cross-striped cabb-7e worm Fou.zrth
(cv 3 se 6x4 ) 2 Southern myworm S i --t h

p~pt-AzOwybis(bengoic acid) Colorado potato beetle Fourth
ROOC j.NNCCross-striped cabbage worm do.
6run 4OHkelon worm Fifth

Barium sulfoleate do. First
DO'(C 16H )>0 2;

33enzalac etophenone( Chal cone) Cabb-age w&e'worm 171, ri
C5C CH0 Colorhiao not to beetle Fourth
C6HCH:HCO6 ~Cross-strired cabbage worm d).
Dian~ondhbick moth do.
Greenhiouse leaf tier Fift'i
Hawaiian beet webworm d.10
Melon worm in.
Southern arMYworm Foirth
Southern beet webworm Fift~l









Table 3-- (Continu=4



Compound Insect Stagel


Benzalacetophenone dibromide Cabbage webworm Fourth
C05CHBrCHBrCOC6H5 Cross-striped cabbage worm do.
Diamondback moth do.
Fall webworm do.
Greenhouse leaf tier Fifth
Hawaiian beet webworm do.
Melon worm do.
Southern armyworm Fourth
Southern beet webworm Fifth


5-Benzalamine-2-cresol Cabbage webworm Third
CR 5CENC H(OR)t Cross-striped cabbage worm Fourth
Diamondback moth do.
Greenhouse leaf tier Fifth
Hawaiian beet webworm do.
Melon worm do.
Southern armyworm Fourth
Southern beet webworm Fifth

p-Benzalaminophenol Cabbage webworm Third
C H CHNC,H-EH Cross-striped cabbage worm Fourth
o 5 o Diamondback moth do.
Fall webworm do.
Greenhouse leaf tier Fifth
Hawaiian beet webworm do.
Melon worm do.
Southern armyworm Fourth
Southern beet webworm Fifth

P,P'-Benzalbis(N,N-dimethylaniline) Colorado potato beetle Fourth
C6H5CH ICO6HN(CH22 Cross-striped cabbage worm do.
Southern armyworm do.

Bn olbis(l1-pyridylamine) Southern armyworm Ffth
,6H CH(C5 3NNH 2
0o 5 53 22
Benzaldehyde phenylhydrazone Cabbage webworm Third
C H5CH:NNHC 6H5 Cross-striped cabbage worm Fourth
Diamondback moth do.
Greenhouse leaf tier Fifth
Hawaiian beet webworm d).
Melon worm do.
Southern armyworm Fourth
Southern beet webworm Fifth









Table 3...(Continued)


Compound Insect staisi/

Benzaldehyde semicarbazone Cross.-striped cabbage worm Fourth
C H CB}INHCORH2 Southern armywors Fifth

9-Benzal fluorene do. Yirst
&C (CHC6H5) CAH

-Ben zal-4--methy1 oxythi anaph then. Imported cabbage worm FoUrth
C~3 H cc(CO)S Southern arulyworm. Thi rl

Bousaxide do. Third

Benzanilide do. do.
C605C00"C 05

Benzeneazo-o-cresol American cockroach 3/4 rown
C.6H9INC H O) CE Cabbage webworu Third
Cross-striped cabbage worm Four th Diamondback moth do.
Greenhouse leaf tier Fifth
Hawaiian beet webworm do.
Melon-worm do.
Rice weevil Adult
Southern armyworm First
do. Fourth
Southern beet webworm Fifth
Termites A&dult
do. do.

Benzeneazoresoreinol Southern arzyworm First
C 6HR5 iC 6H3(OH)2

Benzidire 'do. Third
920CN 2do. Sixth

Benzil do. do.
(C0H5C0)2

AlPha-Benzildioxime Cros&-strlped cabbage worm Fourth
UC)Cio)(65Melon worm Fif th
Southern armyworm Six th

beta-Benzildioxime American cockroach nirst
C6H5C(NOH) C(NOH) C6H5 Cross- striped cabbacje worn Fourth
Melon worm Fiftn
Southern armyworm Sixth






K 2
Table 3.- (Continued)



Corn-ound Insect S4/


gammaa-Benzildioxime Colorado potato beetle Fourth
C I 5C(rO)CNC)C0 5Cross-striped cabbage worm do.
o ~Melon worm Fifthi
Southern armyworm Sixth

Benzilic acid Cross-striped cabbage worm First
(C H ) C(OH)COOH Southern armyworm do.
65 2

alphso1-Benzilmonoxime Cross-striped cabbage worm Fourth
beta-Benzilnonoxime Melon worm Fifth
C6H5C(NOH) COC6H5 Southern armyworm, Si xth

Benzohydrol Colorado potato beetle Fourth
C6H5CH( OH) C 05 Cross-striped cabbage worm do.
Melon worm Fif t
Southern a.rmyworm sixth

alpha-Benzoinoxime American cockroach First
be ta-Benzoinoxime Colorado potato beetle Fourth
C6H5CH( OH) C( NO') C6H5 Cross-striped cabbage worm do.
Southern armyworm Sixth

Benzophenone do. Fourth
Q6,CO C6H5

1-Benzothiazolyl-p-bromobenzyl Colorado potato beetle Fourth
sulfide Cross-striped cabbage worm do.
SOdHONYSC"2C6Hj4r Southern armyworm Sixth

1-Benzo thiazolyl/cyci ohexylaamonium Southern armyworm First
sulfide
EC641SN"3C6H11

1-Benzothiazolyl- p-nitrobenzyl do,. do.
sulfide



Benzothiazyldi sulfide do. Fifth
~C6)S1~S2







853

tble 3.- (Continued)


Compound Insect 3tagei/J


a-Benzotoluide Cabbage webworm Fourth
o-lenzotolulde Colorado potato etle do.
p-Benzotoluidie Crs-striped cabbage wormdo
~3CH~1BCO6E5Diamondback mnoth do.
G'reeaihotxse leaf tier do0.
Hawaiian beet webworm do.
Melon worm do.
Southern armyworm Third
Southern beet webworm Fourth
Yellow woolly bear Sixth

IL-( l-E3ezzoxazolyl )- cyclohexylamine Southern armywo rm Firset


in-Iezoyl-l-suercaptobenzothi~azole Cross-striped cabbage worm Fourthn
SCH4.:SCOC6H5 Southern arniyworm Fi fth

9 -Benzoyl-3-ni trocarbazole do. First


alpha-Benzoyl-betew Cross-striped cabbage worm Fourth
(-nitrophenyletiylene oxide Greenhouse leaf tier Fifth
(~5O~~6H~O2Melon worm do.
Southern armyworm Fourth
Southern beet webworm do.

alphar-Benzoyl-beta-phenyl Cabbage looper Four th
ethylene oxide Cross-striped cabbage worm do.
C5OKKC Greenhouse leaf tier FiftVi
Melon worm d.
Southern armyworm Fourth
Southern beet webworm d10.

3M rltithovanillin Southern armyworm Fi rst


N-Benzylaceteuride Colorado potato beetle Fourth
C6H5CH2HCCE13 Greenhouse leaf tier P~ifth
Hawaiian beet webworm do.
Melon worm Fourth
Southern armyworm do.
Southern beet webworm do.






94

Table 3-.- (Continued)


Compound Insect Stage!/


p-(Benzylamino)-benzenesulfonamide American cockroach First
CH5 c2Nc6HOCHSONH2 Colorado potato beetle Fourth
Cross-striped cabbage worm do.
Melon worm Fifth
Southern armyworm Sixth

n-Benzylbenzamide Colorado potato beetle Fourth
C05CH2NHCOC6H05 Diamondback moth do.
Greenhouse leaf tier do.
Hawaiian beet webworm do.
Melon worm do.
Southern armyworm Third
Southern beet webworm Fourth
Yellow woolly bear Sixth

n-Benzylformamide Colorado potato beetle Fourth
HCONECH C H Greenhouse leaf tier Fifth
5 Hawaiian beet webworm do.
Melon worm Fourth
Southern armnworm do.
Southern beet webworm do.


n-Benzyllauramide Colorado potato beetle Fourth
C11H23CONHCH2C6H5 Greenhouse leaf tier Fifth
Hawaiian beet webworm do.
Melon worm Fourth
Southern armyworm do.
Southern beet webworm do.

Benzylmercaptomannose Southern armyworm First
06H12o(scI 2c6 H5)2

N-Benzylpvlmitamide Colorado potato beetle Fourth
0C1531 CONHCH2C0H5 Greenhouse leaf tier Fifth
Hawaiian beet webworm do.
Melon worm Fourth
Southern armyworm do.
Southern beet webworm do.

n-Benzylpropionamide Colorado potato beetle Fourth
C2pH CONECH2CH5 Greenhouse leaf tier Fifth
Hawaiian beet webworm do.
Melon worm Fourth
Southern armyworm do.
Southern beet webworm do.




854


T&ble 3.- (Continued)


Compound Insect StageY/


Benzylthioxranthic disulfide Cross-striped cabbage worm Fourth~
)1,CCS) sle Southern arnmyworm sixth

B3is(P-bromophenyl)-sulfofle Colorado potato beetle Fou-rth
BC42 o rGreenhouse leaf tier do.
Hawaiian beet webworm, Fifth
Melon worm Fzourth
Southern beet webworm do.

9,9-Bis(l-hydroxy-2-naphthyl)- Greenhouse leaf tier Fifth
fluorene an~by4-ide, Southern armywormFrt


(Other compounds beginnings with "bis" entered under radical that follows.)


Borneol do. Four th
0 1OH17 "

p-Bromobenzenesulfonanilide Colorado potato beetle Fourth
BrC6E0SO HC6H5 Cross-striped cabbage worm do.
Southern arzyworm do.

p-Bromo-N,N-.dibenzylbenzenesulfonamide Colorado potpto beetle Fourth
BrC 40j0S2N( C12C6H5) 2 Cross-striped cabbage worm do.
Melon worm Fif th
Southern armyworm Third

2-Bromo flio rene Cabbage webworm Third
L04?!2fJ3 Br Cross-striped cabbage worm Fourth
Diamondback moth do.
greenhouse leaf tier Fifth
Hawaiian beet webwo)rm do-.
Melon worm Fourtt
Rice weevil Adlt
Southern a rnyw orm Your tn
Southern b'-eet webrcrm Fifth
Termi tee 1 ul t
do. o

2-Bromo-9-.fluorenol Cross-striped ?aba) wrmF rtx
L0H(~OH)903 Br Hawaiian beet webwor Yo t
Velon worm do.
Rice weevil AJ il t
Southern nr-iyuurm yzourth
Southern beet webworu -10.
Termi tes Adul t
do.* do.




......................... .


Table 3.- (Continued)



Ccmpound Insect Sa-l


2-Brcimo-9- fluorenone Cross-striped cabbage worm Fourth
C H COC H Br Melon worm Fifth
6 4 163 Southern armyworm Sixth

p-Bromo-N-methyl-N-phenylbenzenesulf onamide Cross-striped cabbage worm Fourth
BrC6H4SG2N( CH3 )C C65 Melon worm Fif th
Southern arrnyworm sixth

p-Bromo-N-l-naphthylbenzenesulfonamide Colorado potato beetle Fourth
B6HSONC10H Cross-striped cabbage worm do.
Southern armyworm Sixth

2-3romo-7-nitrofluorene Cross-striped cabbage worm Fourth
Br 03H263 N02 Melon worm Fifth
Southern armyworm Sixth

2-Bromo.l-ni tronaphthalene do.* do.
C 10H 7 (N02 )Br,

p-Bromophenoi do. Fourth
BrC6H40H

p-(s-Bromophenyflazo)-phenol Diamondback moth First
BrC 04I":NC6Hj40H Southern armyworm do.

4...(p-Brornophenylazo)-resorcinol Cabbage looper do.
BrC6 H4NNC 6H5(OH)2 Cabbage webworm do.
Cross-striped cabbage worm do.
lxported cabbage worm doe
Melon worm Fifth
Southern armyworm First
do. Sixth
~4-(p-Bromophenylazo)-5, 6, 7,8-tetrahydro- Bean leaf roller First
l-.naphthol Cabbage looper Second
BrC 6H 0:C10H Diamondback moth First
Imported cabbage worm do.'
Southern armyworm do.
do. Fourth
2-Bromo,-5-phenyl-2, 3-cyclohexenone do. First
Br?: ZCH~CHH( CcH )CH1 :
9 2Y :










.1








Table 3..(Continued)


Compound Insect Sae.


N-p-Brornophenylsulfonyvl- Colorado potato beetle -r
mrnrholine Cross-strined ca rm do.
BrC HIS02,N(H CH ) 20 Southern armywo-rm, Thirad

2, 3-Butanedione-3-nonoxime Colorado potato beetle Fourth
CH 3 OC(NH)CH Cross-striped cabbie worm do.
3 3Southern armyworm do.

Batyl allophaziate do. First
XK2CO 2C449

N-nk-Thtyl-p- toluene sulfonamide Diamondback moth Fourth
M CIEHS2NHC4Hq Greenhouse leaf tier do.
Hawaiian beet webworn Fifth
Southern armyworm Fourth
Southern bee t webworm Fif th

CalciUM salt of chlorinated sulfoleic acid Colorado potato beetle Fourth
Greenhouse leaf tier do.
Hawaiian beet webworm Fifth
Melon worm V'our th
Southern armyworm Third
Southern beet webworm Tourth
Calcium sulfoleate Southern armyworm First
Ca( C18,H3SO2) 2

N-(o>-Carboxyphenyl)glycane Cross-striped cabbage worm do.
EO0OC6H04NHOH2C00H Southern armywora do.

Catechol do. Sixth
C6H4(cH)2

Ohloroacetyldiphenylami ne do. Thirl
CH2 C1 OC 6 H))41C 6 R5

2-Chljoroacridone Cross-striped cabbage worm First
)4-Chloroacridone Imported cabbage worm do.
M~CcH1-"CJ6H3CJ. Southern armyivorni do.
l Clr--mn--ihnlmn do. C1.
C 6H5 NHC6H3 CJNH 2 Sixth

(4-Okhloro-2-aiinophenylmercapto>..acetic Cross-striped cabba(-e worm Fourth
acid Southern arniyworm Sixth
Cl1%H3N&2) 50H2 OOH








Table 3.--( Continued)


Com-oound Insect Sasl


alpha- (p-Chloro'oenzoyl)-beta-(m- Cross-stripoed cabbage worm Four th
nitro~henvl) ethylene oxide Greenhouse leaf tier Fifth
C).C6F-4COEHHC00j.N2 Melon worm do.
Southern armyworm Four th
Southern beet webworm do.

almha-(p,-Chlorobenzoyl)-beta-phen,-l Southern armyworm First
ethylene oxide


3-C hio rocar'bazole do.* do.
03 6H C1 do. Fifth

2-Chloro-3,5-dinitrobenzoic acid Cross-striped cabbage worm Fourth
'.lS6R2(NO2) 2~~o Southern armyworm Fif th

21-Chlorodiphenylamine-2-carboxylic acid do. Fifth
3 -Chlorodiphenylamine-2-carboxylic acid
ClC6H4'THC6E4COOH

9-Chlo rofluo rene Colorado potato beetle Fourth
Cross-striped cabb-ge worn d.
Southem annyworm sixth

6-C.'hlori 2-methy2.-l ,4,2-benzothiazine- Southern armyworm First
3(4I)-onae do. Sixth



2-Chloro-4-nritroaxiline American cockroach 3/4& grown02C 73 N V Diamondback moth Four th
Greenhouse leaf tier Fifth
Hawaiian beet webworm do.
Melon worm Fourth
Rice weevil Adult
Southern arinyworm Third
do. sixth
Southern beet webworm Fifth
Termites Adult
do. do.

4-Choro-2-nitrodiphenylainine Cross-striped cabbage worm First.
C 6 H NHC 6H 3Ci1o do. Second
65 63do. Third
do.* Fourth
Diamondback moth First
do. Secopid
Imported cabbage worm First
Southern armyworm do.
do. -Second
do. kw





99
Table 3--(Continued)


Compound Insect

2-Chloro-7-nitrofluorene Colorado potato beetle Fourth
NOPCt6"1'CF2C6H4C1 Cross-striDed cabbage ;7orm, First
'Imported cabbage worm. d-).
Southern arT,-.,yworm d,3.

14-Chloro-2a-nitrophenyl eater of Diamondback moth do.
thl-ocvanic acid Southern arryworm do.
Cie 6 H 3 (NO 2 )SCN

(4-Chloro-2-nitro-ohenylmercapto)-acetic Cross-strined cgL'hba7e worm Fourt)h
acid Southern armyrorr, Fif td
Me 6 H 3 (NO 2 )SCH 2 COOH

alpha-(4-Chloro-P-r.itroplu-erylmercapto)- do. do.
acetophenone
Cie &3 SCH2,;Cc b5

4-Obloro-P-ni tronheryl sulfurm.tne Cross-strir)ed cabbage worr, Fourth
Me 03 (N02)SNH2 Southern armyworm Fifth

4-Chloro-2-nitrophenyl sulfur do. do.
bromide
Cleo 3 (NO 2) SBr

4-Chloro-ikenaziminobenzene do. Sixth
C5 C6H5
0-Chlorophenyl est. ,r of Colorado Dotato beetle Foi ,rth
pl-toluenesulfonic acid Cross-striped cabbage worm do.
P-Chlorophenyl ester of Southern armyworm Sixth
pl-toluenesulfonic acid
Cic 6 H 40SO 2C6 H 4CH7

4-Chloro-m-tolyl ester of Colorado pot,-to b,,-tle
pl-toluenesulfonic acid Cross-striped
ClC6H 3 (CH 3 )OSO 2 C 6 H 4 CH 3 Southern anywo rm Th i

p-Chloropheny! furfuralmethyl ketone do. F]L tn
CH:CHCOC HIM
(C030) 6 +
Chrysene do. Vj
C Hin
19 C
Chrysyl&,,Ane
C19H 11"'32






90
Table C-oatinued)



Compound Insect Stagel/


m>Cresyl furoate Southern armyworm Fifth
(Co4 H 3o)COOC 6 H3(H H3 )OH

Cyanuric acid do. First
HO9:NC( OH) :NC(OH):

2- (alpha- (2-Hydroxy:-6-oxo-4 ,4-dimethyl- do.* do.
dleltal-cyclohexenyl)-ethyl)

(CH 3) 2C C2COHCO2


cocH2c(C cH)2CHCO

2- ( 2-Hyiroxy- 6- oxo-I14- dime thyl-del tal- do. do.
cyclohexenylmethyl )-5 ,5-dime thyl1, 3-cyclohexanediione
oO2C OH) 2 O2co 2cO c c3) ~2 OR

n- Cyc2.oh:!Ylacetarmide Colorado potato beetle Fourth
CON2 Southern -,rmyworm do.
3 l

n-Cyclolhe,,:J berzamide Cross-striped cabbage worm do.
1E CO H 11I Southern armywo m, ~ Fifth


n- Cyclohei. ,' i.,rami de Hawaiian beet rebworm dIO.
ClH 'CHMelon worm Fourth
2 611Southern armywoi do.
Southern beet webworm do.
Yellow woolly bear do.

n-Ccloe~ypaiitaideHawaiian beet webworm Fifth
15 31c '06H 11Melon worm Fourth
Southern armywom do.
Southern beet ,vebworm do.
Yellow woolly bear do.

o- Cyclohexylphenol Southern arm.yworm First
C6H11C0614OH do. Third
do. Fifth

o- ycohxylheolColorado potato beetle Fourth
HOC06HkCH1 do. do.
Cross-striped cabbage-worm do.
Fall webwormFit
Southern armyworm First
do. Sixth





91

Table 3-4Continuei)


Compound Insect Stage!/


N-Cyclohexylrponmd Hawaiian beet webworn Fifth
C 2H CON~C 6H 11Melon worm o:rt
25Southern armyworm io.
Southern beet webworm do.
Yellow woolly bearx do.

1, 9-Diaminonaphthal ene Colorado -potato beetle Fosurth
C 10H (NH 2) 2Cross- stipedi cabbage worm o
Melon worm FZif't
Southern arimy"iorm Fou rth
do. Sixth

2, 3-Diaminophenazine do. Fir3t
C6Hj402C6H2(NH2) 2 do. Sixth

Diani salcyclopentanone American cockroach 3/ crown
3H 0 0 CH O'?0 elon worm Fourth
3 6H~*CcdHcH2( ~~PVSouthern armywo rm Fifth
Southern beet webworm do0.

Dibenzodtoxin Colorado potato beetle Fourth
?64C0?Cross-striped cabbage .7orm do).
Melon worm Fifthj
Southern armyworm First
do. sixth

Dibenzalcyclopentanone Hawaiian beet webworm, Fifth
CGHOHcHcHC(cHCH5?0Melon worm Fourth
C65HFHC2(:H0%oSouthern armyworm do.
Southern beet web'icrL Fifth

2. 2.,,4-Dibenzophenazine Southern annyworm First
?HiNNC4H,_Q

flibenzopheno thioxin dio. Fiftq~
S!OO H __210 6

2,3,6.7-Dibenzoxanthone Coloraao potato boetle Folirt1.
0C IiCross-striped cabb, je w. rm, Fi r.sZt
1 10 6Imported cabbage worm


p-Dibromdiphenyl SolitL-,-rn .=-.yworm
BrC6H4C 6H41Br

9, lO-Dibrornoanthracene do. .
C04~(0Cr) 206H41






92

Table 3.- (Continued)



Compound InsectSte/


2, 7-Dibromo-O-benzaJA'luorene Southern armyworm First
Br q6fH3C( CCH) C6H3Br

alpha, alpha'-Dibronaobibenzyl Colorado potato beetle Fourth
(stilbene dibromide) Cross-striped cabbage worm do.
C0H5CHBrCRBrC6H5 ,/ Southern armyworm Sixth

2, 7-fibromo- ( o-chlorobenzal.)-fluorene do. First
Br 6H C(aC6HCl)?6 63 Br

Dibromo-o.cresosulfonphtn ein Southern armyworm do.


~,> b~- 3 I-qro--n~e olorado potato beetle Fourth
CCEC~~rCi~COCi~Cross:-striped cabbage worm do.
Southe rn arriyworm Sixth 2,,:>rnfurn Southern armyworm First






~1pa ea-Dibomhydocnxi~i acd.Colorado potato beetle Fourth
sY~. OGH- ro stripped cabbcnge worm do.

2?Jo--- ,inyl--butanone Colorado potato beetle do.
CWI~rCOCHCross-striped cabbage wormdo
3Saut_ ern armyworm sixth

4 ~Crossz-striped cabbage worm Fourth
7 -~ ,: elonr worm Fifth
S-1 t,-ern armyW')rn :31x3th
Di ~}~yir~ourea, Crosb-dtriped cabbage worm Fourth
'> NSou tr n ar. ",orm Fifth

p, P Dcii, yr 7ene do. do.



P-Dichloro'benzene Cross-striped cabbage worm Fourth
Ci lSouthern aruiywrm Fifth
4,1Di loro-?2' cdinitrobiF, 1iy Colorado potato beetle Fourth
C1 (No2) C6H4C6(No2)Cl Cross-striped cabbage worm do.
Melon worm Fifth
Southern arayworm Sixth






93


Table 3--(UontizuPd)


Compound Insect StageV

2,7-Dichlorofluorens Cross-striped cabbage worm First
C1 693 Cl do. Fourth
Diamondback moth do.
Greenhouse leaf tier do.
Hawaiian beet webworm Fif th
Imported cabbage worm First
Melon worm Four th
South m armyworm First
do. Fourth
Southern beet webworm Fifth

1-(3-,5-Dichlorc -2-hydroxyphen.viazo)- Southern armyworm First
2-naphthol do. Thirl.
Cl2C1h(OH)':NClOH60R

Vichlorophenol sul fonphthalein do. First
ban
E-2-COO: ( C03 Cl 2(X) 2

6-(2 9-n1eh1or*phsayl&s*)- Cross-striped cablowe woru Fourth
oro-wcre'sol Southerii ainyworm do.
C12003 N:NC 02 ( I (Z 3)(Cl)OK

2-(2 chloraphanylazo)- Cross-ictriped cabbage worn do.
9%:orothymol Southern ar"wo ra do.
C12C6H :NC'WGH(Cl)(CH3)(OR)CH(CH3)2

4-(2,5--Dichlorophonylazo)- Cabbage looper First
*-cresol Cabbage webworm do.
C12C6H3l:NC6R3(CE3)00 Cross-striped cabbage wors do.
Diamondback moth do .
Southern armyworm

2-(2.5-Dichlorophanylazo)- Cross-striped cabbage worm Fo" r
p-cresol Southern armyworm, do.
Cl2o6H3N:NC03 (CH3)CR

1 -(2,5-Dichlorophenylazo)- Cabbftge looper Yirst
o-cycloho371phonol Cabbage webworm do.
C1 :NC Cross-striped cabbage worm do.
2CO? 03(coll)c" Diamondbr-c1c moth 10.
Imported cabbage worm
Southern armyworm
do.








914
Table 3.- (Continued)


Compound Insect StW4e1-(2,5-Dichlorophenylazo)-2-naphthol Cross-striped cabbage worm Fourth
4- (2, 5-Dichlorophenylazo)-1-flaphthol Southern arwyworm do.
C 2C 6H3N:NC 10H6OK

(4-(2,5-Dichlorophenyla7.o)-l- Cross-striped cabbage worm do.
naphthylmethyl ether Southern armywiorm do.
Cl ?_C 6 H3N:NC 10H 6 OOH3

p-( 2, 5-Dichlorophenylazo)-phenol do. Sixth
Cl C H NNCH OK

~4-(2, 5--Dicrlorophenylazo)-resorcinol Oabbae looper First
C2 6 3NT673(OH)2 Cabbage webwormdo
Cross-striped cabbage worm do.
Southern armyworm do.

4-(2,5-Dichlorophenylazo)-thymol Cross-striped cabbage worm Fourth
Hl203N 2 (CH 3)(QH)OH(CH 3)2 Southern armyworm do.

4-(2, 5-Lichlorophenylazo)-2,5-xylenol Cross-striped cabbage worm do.
Cl2COH5N:NC6 H2( CH3) 20H Southern armyworm do.

K -(2. 5-Dichlorophenylazo)-2, -xylenol do. First
1' 2 06O3N ;NC6TT2( GE3) 20H

2,4-lDichlorophenyl ester of Colorado potato beetle Fourth
31,4-dichlorobenzenesulfonic acid Cross-striped cabbage worm do.
C12C6H20S02C6H3C12 Southern arrnyworm Sixth

20KDic-hlorophenyl ester of pl- Colorado potato beetle Fourth
toluenesulfonic acid Cross-striped cabbage worm do-.
C2 C6 H3 Clo2 06 H 3 Southern armyworm Third

_,-3s( ldichlorophenyl)-triazene Cross-striped cabbage worm Fourth
(Cl2C6H 4i C3HN31 Southern armyworm do.

Di-m-cresyl carbonate Southern armyworm First
Di-o-cresyl car~bonate
Di-ui-cresyl carbonate
(ROCK 3 C6B3)2CO3

Di.cyariodi amide Colorado potato beetle Fourth
HN; C(NH 2)NE(H Cross-striped cabbage worm First
Fall webworm Fifth
Imported cabbage worm First
Souths-rn armyworm do.






95

Table 3.- (".outinuea)


Compound Insect Stage.-2.5-I)cyclopentylidene- Colorado potato beetle Fourth
cyclopentanone Diamondback moth %..
(C 5%) 205H 40 Greenhouse leaf tier Fifta
Hawaiian beet webworm do.
Melon worm Fourth
South -rn 8.r-yworm o
Southern beet webworm do.
Yellow woolly bear Sixth

Diethyl ester of ethylenediamine- Cross-striped cabbage worm First
N,Nt1--beta,beta'l-bie(crotonic acid) Southern armyworm do.
(C2X5ococE6C(CH3)N'~272

N, N-Di.ethyl-2-naphthalenesulfonanide American c ockroach do.
C H so2(~) Cross-striped cabbage worm Fourth
1072(252Melon worm Fifth
Southern aruiyworm Sixth

N,N-Diethyl-p-nitrosoaniline Cabbage looper Fifth
OZNCrEbI(c C~~2 Colorad potato beetle Fourth
Cross-striped cabbage worm do.
Melon worm Fifth
Southern armyworm Fourth

Di furalcyclopentanone Southern armyworm First
C 15RNO 3

9,10-Dihydroanthracene Cross-striped cabbage worm Fourth
C 6R4( CH)2 C 6H1, Melon worm Fifth
2 ~Southern armyworm Sixth

2.-iyrqiiie1 royi acid American cockroach 3/14 -rown
?04~C(C00H)' VLHP2 2d Melon worm Fourth
2Southern armnyworm Fifth
Southern beet webworm do.


297-Dihydroxynaphthalene Colorado potato beetle Fowrth
HOC 1016OH Cross-striped cabbage worm do.
10 6Southern arnyworm do.


9,..i~..ydo.rpeyl)-fltzorene Colorado potpto beetle .
do0.
6H14C(COH4OH' 2?0Hj Cross-striped c '4babh47e w-,rm
Southern --r; \vv- r-,nSit




................. .......




Tabie 3.--(Continued) 96

Ccumoxmd Insect
PPt-Diiodoa:;oxybenzene Cross-striped cabbage woru Fourth
IC644nC6"4I Melon worm Fifth
Southern armUmrs do.

i)-A)Uodobenzene Cross-striped cabbage worm Fourth
C Southern arzWwra First
6H4,2 db. sixth
PD'-Diiodo.inherv1 do. First
IC 04CO4,

2,6-D1iodo-4-nitro&nilin9 do. do.
H
I 2C 6" 2
DI-P-methoxydiphenylamine do. doe
OH.3OC6'Y RC6"40C%

p-Dimethylaminobenzaldehyde do. do.
(CH 3YE6 H 4 CHD eo. sixth

D-Dimethylaminoazobenzene do. First
(CR 3)2 C6HO:'KC6H5

4-Dimethylaminobenzene-1-azo- do. do.
1-naphthalene
4-Dtmethylaminobenzene-l-aro2-na-ohthalene
CH3) 2 CO41': "C10'17

p, '-Bis(dimet-ylamino)-benzoplienone Greenhouse leaf tier Fourth
(CH Go Hawaiian beet webworm Fifth
3)2;'C6H]2 Melon worm Fourth
Southern armyworm ftird-.
Southern beet webworm Fourth

o-(p-D1methylaminophenylazo)- Southern armyworm First
benzoic acid
OR
3YO6% :NC04000H
alphaalpha -P1s((p-(N,1T-dimethylamJLno)- Colorado potato beetle Fourth
phe;iyl)) --o-cresol Southern armyworm Third
CH 3) 2P6 q 2 CHC6H40H

alpha. alpha-Bi s((p-(J6T-dimethvlamino)- Colorado potato beetle Fourth
,phenyl))-p-methylanisole Cross-striped cabbp,-e worm do.
CH3)2KC6H] 2CHC6H40CH3 Southern armWvorm Third

p-Dimgthylamino-ohenyl-l- Cross-striped cabbage worm First
naphthoquinorimine Southern armyvorm do.
CH3) 2 C6%"l C 1%60
lCr






97
Table 3.-(Continued)


Compound InsectSteI


Bi8(p..dimethylamincphenyl) sulfide Cross-striped cabbage wzorm First
1iH O3) 2NCbH4] 2 S Imported cabbage worm do.
Southo'rn arnyworm do.

5,5-Dimethyl-1, 3-cyclohexanedione do. do.
F2CC 2CC 21(3 )2

W,N-Dimethyl-p-toluenesulfonazaide Colorado potato beetle Fourth
CH 3 C6H0,S%( CH.3)2 Cross-striped cabbag-e -Normdo
~, 2Melon worm Fifth
Southern armyworm Fourth

be ta-Dinaphtho furan do. Fifth


Dinaphthyl thiourea &o. First
(c10u. N) 2 Cs

p-(2,4-Diitroanilino)-phenol Colorado Potato beetle Fourth
HoC NEuC RH(NO ) Cross-striped cabbage worm do.
6 6 3 22 Southe rn armyworm Sixth

O-Dini trobenu do. First
06R4~(102)2, do. Third

~4,E-Dinitro-o-.cresol methyl do. Fifth
ether
(NO 2) 200H2(C"H3) OCH 3

0,90 I-Dini trodiphenyl do. do.
NO2 C6H1 6H402

2, 4-Di ni tro aj~nylamnine Colorado pott el
C 6HC6H(No )2 Southern -ar-vywr I

o ,o -Dini trodiphenylamine do.
NO 2C6HRC6O2

4,1-Dinitroiphenyl sulfide CrF-t~e u'~~r~
(No 2CO6H)S

2, 7-Dini trofluorene o
NO 2 ?H 26 H3 N02 Melon worm
Southern armnyw arc







98

Table 3.-- (Continued)


Compound Insect Stagei


1,5-Dinitronaph.thalene Cabbage looper First
C 10H6(N02) Colorado potato beetle Fourth
Cross-striped cabbage worm First
Imported cabbage worm do.
Southern armyworm do.

1,9-Dinitronaphthalene Cabbage looper do.
C 106(NO 2) Cross-striped cabbage worm do.
106 22 do. Third
Imported cabbage worm First
Melon worm Fifth
Southern armyworm First
do. Third

3,5-Dinitrophenoxazine Cross-striped cabbage worm First
nE 2(NO2 Imported cabbage worm do.
__ _2 2)2 Southern armyworm do.

Di-o-nitrophenyl disulfide Cross-striped cabbage worm Fourth
NO2 $6 4SCoH4NOR Diamondbe.ck moth do.
Greenhouse leaf tier do.
Hawaiian beet webworm Fifth
Melon worm Fourth
Southern armyworm First
do. Fourth
Southern beet webworm Fifth

Di-p-nitrophenyl dieulfide Southern armyworm First
NO2C6HkSSC6H4NO2

4-(2, 4-Dinitrophenyl)-morpholine Cross-striped cabbage worm Fourth
(NO2) 2 C6H3N(CH2CH2) 20 Melon worm Fifth
Southern armyworm do.

D1-Y.-aitrophenyljsulfone Colorado potato beetle Fourth
N2C6H4S02C6HNO2 Cross-striped cabbage worm do.
Melon worm Fifth
Southern armyworm do.

N'-NDinitroso-N,N'-diphenyl- Colorado potato beetle Fourth
p-phenylenediamine Cross-striped cabbage worm do.
C6H N(NO)C6H 4N(NO)C6H5 Southern armyworm Sixth

DiCzin bh0 lenethiophene Colorado potato beetle Fourth
10oH6GSCOIH6 Cross-striped cabbage worm do.
Melon worm Fifth
Southern armyworm Sixth






99

Table 3.- (Continued)


Compound Insect


m-Diphenylbens~ehe Southern arinyworm it
o-Diphenylbenz ene do. Third
p-Diphenylbenzene
CH5 C6Hj'C65

Diphenylchlaroacetic acid Cross-striped cabbage worm~ First
(C H) N CClCOOHT Southern arimyworm do.

Diphenylene disulfide Cross-striped cabbage worm Four-th
(004)2S2 Diamondback '~Tith do.
Greenhouse leaf tier Fif th
Hawaiian beet webworm. do.
Melon worm Fourth
Southern arm"y-wo rm do.
Southern beet webworm Fifth

Diphenylethylenediamine Southern armyworm First
(C6H51HCH2) 2

N,NO-Diphenylfornamlidine Coloradio potato beetle Fourth
COH5NMC-flH6 Cross-striped cabbage worm do.5 )Southern ar,nyworm do.

aloha, gam-Dipenyl guani di ne Colo rado potato beetle do.
C65BC(N)NEfCOH5 Southern armyworm Sixth

Diphenyj~methlene. do. Fifth
dithio- colicc acid


Diphenyl-p-phenylenediamine do. Fir*t
C 0HfC0H1MC 6 H5 do. Sixth

1.4-Diphenylpiperazine Colorado potato beetle Fourth
C0H5 i(CH2CH2)2NC6H5 Cos-strip~ed cabbage worm do.
Southe rn armywo rm Third

Di henylpyri dylamin. do. do.
0C5H)4N)N(C 6H5)2

Diphenylpyridyl-uanidine do.do
(C6H5INH)2C:N(CH4N)

2, 3-Diphenylquinoxaline do. F1 rnt
C H N;C(C R )-(C H ) N







100

Table .A Continued)


Compound Insect stagl.'


4,4-Diphenyleemicarbazide 'Colorado potato beetle Fourth
(C65) 2NC0NHEH2 Cross-striped cabbage worm do.
Melon worm do.
Southern armyworm Third

Diphenythiocar-bazide Cross-striped cabbage worm Fourth
C 13R1 N 4S Southern armyworm Fifth


P4Diphenylthiophene Cross-striped cabbage worm First
C6H ~CC6H) ~Imported cabbage worm do.
'C HSouthern arinyworm do.

symDihenltioueaCross-striDed cabb1-age worm Fourth
(O6~~~2CSSouthern ariIVworin Fif th

~- ~LpbyJ ~reaColoradio potato beetle Four th
CCH ross-striped cabbage worm do.
o5 ~Melon worm FMft
Southern armyworm Third

ipipe<~<~~c ~American cocroac 3/4 grown
qeE ~~D \)(!rHCEOC H2 Melon worm Fourth
___ -Southern armyworm Fifth
Southern beat webtworm do.


Dip; ~Cross-stripel cabbage worm Fourth
(C~J4Th j~Southern armyworm Fifth

alIpha-,al'pba,-Di-oyridylthiourea Cross-striped cabbage worm Fourth
C1 11Southern axmyworm Fif th
_IC. 4

betaj KJ'r>Ylthiourea Cross-striped cabbage worm Fourth
I-ISouthern armyworm Third

1~N D cI~ei~e2.o~amaeCabbage looper First
HOC 6H,1JCH:'CT12Ch2K: aeC674oH Cross-striped cabbage worm do.
Southern armyworm do,
do. Third
do. Sixth

D13odium I-slfsridophenyl-2-azo- Colorado potato beetle Four th
7- ac etam i n o-l-hydrorynaph thal ene- Cross-striped cabbage worm First
3, -disul f onat e Southern arnyworm do.
(Naso 2 C 10EH (NHCOCH )(0H)NC 6 H 4 SO 2NH do. Fourth


32103 5A